No (12575)
Number of found documents:
12575
Published from
to
CE-MS separation and identification of standard nucleotides
Butnariu, Maria; Šolínová, Veronika; Koval, Dušan
2022 - English
Keywords:
capillary electrophoresis; mass spectrometry; nucleotides
Available at various institutes of the ASCR
CE-MS separation and identification of standard nucleotides
Vibration mode shape extraction of bladed disk
Mekhalfia, Mohammed Lamine; Procházka, Pavel; Tchawou Tchuisseu, Eder Batista; Maturkanič, Dušan; Hodboď, Robert
2022 - English
This research paper deals with the experimental protocol followed to visualize the vibration mode shape of an aero-engine bladed disk. This study is based on a comparison between the numerical results obtained through Finite element methods (FEM) using ANSYS software and experimentally using the laser Doppler vibrometer. Therefore the bladed disk was transformed into a 3D virtual environment and structural analysis was performed. The results demonstrate a match between the numerical and the experimental one, this match offers the possibility for using the model for future studies.
Keywords:
blade disk; mode shapes; laser doppler vibrometer
Available at various institutes of the ASCR
Vibration mode shape extraction of bladed disk
This research paper deals with the experimental protocol followed to visualize the vibration mode shape of an aero-engine bladed disk. This study is based on a comparison between the numerical results ...
Approaches to dynamical analysis of rotors with parameters of uncertain magnitudes
Zapoměl, Jaroslav; Kozánek, Jan; Košina, Jan; Cibulka, Jan
2022 - English
In many cases, the rotor configuration or loading characteristics are described by parameters of uncertain magnitude. Several procedures were developed to analyse such systems. This paper deals with the approach based on application of the fuzzy numbers. The investigated mechanical system is a rotor supported by hydrodynamic bearings. The parameters of its loading have uncertain values.
Keywords:
rotors; uncertain parameters; fuzzy numbers approach
Available at various institutes of the ASCR
Approaches to dynamical analysis of rotors with parameters of uncertain magnitudes
In many cases, the rotor configuration or loading characteristics are described by parameters of uncertain magnitude. Several procedures were developed to analyse such systems. This paper deals with ...
Turbine blade linkages in reduced modal synthesis model
Pešek, Luděk; Šnábl, Pavel
2022 - English
The paper is the first stage of our modelling turbine blade linkages in reduced modal synthesis model. The modal synthesis method is used for the dynamic behaviour studies of turbine bladed wheels with frictional inter-blade linkages and in case of the microslips the stiffening effect of the linkages play an important role in wheel dynamics. The paper presents the first results of modal analysis of the wheel when springs were used to substitute the linkages in the modal synthesis model.
Keywords:
bladed wheel; reduced model; tie-boss; shroud; stiffening
Available at various institutes of the ASCR
Turbine blade linkages in reduced modal synthesis model
The paper is the first stage of our modelling turbine blade linkages in reduced modal synthesis model. The modal synthesis method is used for the dynamic behaviour studies of turbine bladed wheels ...
Aeroacoustic Noise Source Investigation in the Case of the Blade Cascade
Procházka, Pavel P.; Antoš, Pavel; Šnábl, Pavel
2022 - English
The blade cascade consisted of five NACA 0010 profiles is examined in the framework of project dealing with nonlinear dynamic phenomenon related to stall flutter of flexible profiles with pitch degree of freedom in subsonic flow. Various angles of attack (AoA) of the cascade generates different (broadband) aeroacoustic noise. The goal of this article is to describe the existence of possible noise sources using two experimental methods – Particle Image velocimetry (PIV) and hot-wire (HW) anemometry.
Keywords:
blade cascade; time-resolved PIV; HW anemometry; FFT
Available at various institutes of the ASCR
Aeroacoustic Noise Source Investigation in the Case of the Blade Cascade
The blade cascade consisted of five NACA 0010 profiles is examined in the framework of project dealing with nonlinear dynamic phenomenon related to stall flutter of flexible profiles with pitch ...
Temporal, Spatial, and Spatio-temporal correlation of the velocity fluctuations
Jurčáková, Klára
2022 - English
Taylor's hypothesis about frozen turbulence [1] says that if the turbulence intensity is small compared to the mean velocity then the advection of a turbulent flow field past a fixed point can be taken entirely due to the mean flow. This means that in the “frozen turbulent field” spatial and temporal dimensions can be interchanged. Although the main assumption of Taylor's hypothesis is not met in the atmospheric boundary layer (the intensity of turbulence is usually between 10 and 20%) the hypothesis is commonly used to calculate integral length scales of turbulent fields from point measurements. Particle image velocimetry with high temporal resolution (TR-PIV) allows us to analyze both temporal and spatial cross-correlations in the turbulent flow fields and to evaluate obtained results.
Keywords:
frozen turbulence; wind tunnel; integral length scales; Particle Image Velocimetry
Available at various institutes of the ASCR
Temporal, Spatial, and Spatio-temporal correlation of the velocity fluctuations
Taylor's hypothesis about frozen turbulence [1] says that if the turbulence intensity is small compared to the mean velocity then the advection of a turbulent flow field past a fixed point can be ...
Inverse-Heusler Mn2FeSi alloy prepared by powder metallurgy route
Životský, O.; Skotnicová, K.; Čegan, T.; Juřica, J.; Gembalová, L.; Zažímal, František; Jirásková, Yvonna; Szurman, I.
2022 - English
The Mn2FeSi inverse-Heusler alloy was prepared by solid-state reactions using ball milling for 168 h in n hexane. Two milling procedures varying in the ball-to-powder ratio, namely 4:1 and 10:1, were used to follow \ntheir influence on alloy formation and its physical properties. In both cases no Heusler structure was obtained \ndirectly and therefore the subsequent annealing at 1223 K for 1.5 h in pure Ar was applied. The energy dispersive X-ray analysis resulted in the chemical composition about 49.0-49.9 at% Mn, 25.3-25.6 at% Fe, and \n24.8-25.4 at% Si, in a good agreement with nominal one. X-ray diffraction of both powders confirmed inverse Heusler XA structure of lattice parameters 0.5675 nm (4:1) and 0.5677 nm (10:1), only slightly higher as \ntheoretically obtained 0.560 nm. The presence of minor oxidation phases was also observed in the particle \nstructure of powders. Magnetic properties were analysed at low and room temperatures. Both alloys exhibit \nparamagnetic behaviour at room temperature confirmed by transmission Mössbauer spectroscopy \nmeasurements. Different magnetic behaviour of alloys is observed below 65 K.
Keywords:
Heusler alloy, powder, ball milling, microstructure, magnetism; powder; ball milling; microstructure; magnetism
Available at various institutes of the ASCR
Inverse-Heusler Mn2FeSi alloy prepared by powder metallurgy route
The Mn2FeSi inverse-Heusler alloy was prepared by solid-state reactions using ball milling for 168 h in n hexane. Two milling procedures varying in the ball-to-powder ratio, namely 4:1 and 10:1, were ...
NANOCERIA PREPARED BY ELECTRON BEAM EVAPORATION
Pizúrová, Naděžda; Hlaváček, A.; Kavčiaková, Zuzana; Roupcová, Pavla; Kuběna, Ivo; Buršík, Jiří; Sokovnin, S. Y.
2022 - English
Cerium oxide nanoparticles (nanoceria) are currently one of the most investigated nanomaterials because of their attractive properties used in biomedical applications, catalysis, fuel cells, and many others. These attractive properties are connected with the Ce3+ and Ce4+ valency state ratio. In the nanoparticle form, cerium oxides contain a mixture of Ce3+ and Ce4+ on the nanoparticle surfaces. Switching between these two states requires oxygen vacancies. Therefore, nanoceria's inherent ability to act as an antioxidant in an environmentally-dependent manner and a “redox switch” to confer auto-regenerating capabilities by automatically shifting between Ce4+ and Ce3+ oxidation states is significantly affected by surface morphology. Regarding this demanded behavior, we aimed to characterize synthesized nanoparticle surface quality and its influence on the cerium oxidation states. The received results were used to evaluate the synthesis method's suitability for suggested utilization. We used nanoparticles prepared by electron beam evaporation. This unique physical method includes nanoparticle creation through the fast cooling process followed by breaking radiation damaging nanoparticle surfaces to create surface off-stoichiometry. We prepared a sample containing clusters of a mixture of ultra-small nanoparticles and approximately 100 nm particles. X-ray diffraction confirmed the CeO2 phase in both components. To extract the finest component, we used centrifugal size fractionation. We received 200 nm clusters of 2-10 nm nanoparticles. Nanoparticle shapes and facet types were analyzed using transmission electron microscopy methods. We found out most nanoparticles were formed with truncated octahedrons containing {1,1,1} and {1,0,0} facet types and truncated cuboctahedrons containing {1,1,1}, {1,0,0}, and additional {1,1,0} facets. No octahedron (without truncation) containing only {1,1,1} facets was observed. Nanoparticle shapes containing {1,1,0} and {1,0,0} are suitable for redox activity. Some amount of irregular shapes, beneficial for redox activity, was also observed. Spectroscopy methods confirmed Ce3+ content.
Keywords:
Ce3+ and Ce4+; electron beam evaporation; facet types; hrtem; Nanoceria
Available at various institutes of the ASCR
NANOCERIA PREPARED BY ELECTRON BEAM EVAPORATION
Cerium oxide nanoparticles (nanoceria) are currently one of the most investigated nanomaterials because of their attractive properties used in biomedical applications, catalysis, fuel cells, and many ...
INFLUENCE OF THE DEPOSITION PARAMETERS ON MICROSTRUCTURE AND PROPERTIES OF HVOF SPRAYED WC-CRC-NI COATING
Vražina, Tomáš; Šulák, Ivo; Poloprudský, Jakub; Zábranský, K.; Gejdoš, P.; Hadraba, Hynek; Čelko, L.
2022 - English
This paper investigates the influence of thermal spray parameters of the high-velocity oxygen fuel (HVOF) process on the properties of cermet coatings prepared from commercially available Amperit 551 WC-CrC-Ni powder. Three different processing parameters were applied to optimize the production process with the aim to achieve preeminent mechanical properties and fully dense material without microstructural defects. The deposition was carried out by a GLC5 gun. The velocity and temperature of powder particles in the spray stream were monitored by Accuraspray Tecnar diagnostic tool. The quality of deposited coatings was analyzed by means of light microscopy, scanning electron microscopy, and X-ray diffraction. The chemical composition of the used powder and sprayed WC-CrC-Ni coating was determined by energy dispersive spectroscopy. It was found that the spray parameters have a negligible effect on the resulting microstructure and phase composition of the coating. However, the porosity and surface roughness were significantly affected by the variation in process parameters. To assess the basic mechanical properties of HVOF sprayed coating instrumented Vickers hardness measurements were utilized. The coating hardness reached mean values over 1400 HV 0.1 and the indentation modulus varied from 152-279 GPa.
Keywords:
hvof; microhardness; WC-CrC-Ni
Available at various institutes of the ASCR
INFLUENCE OF THE DEPOSITION PARAMETERS ON MICROSTRUCTURE AND PROPERTIES OF HVOF SPRAYED WC-CRC-NI COATING
This paper investigates the influence of thermal spray parameters of the high-velocity oxygen fuel (HVOF) process on the properties of cermet coatings prepared from commercially available Amperit 551 ...
Electrochemical Techniques in Monitoring of Nervous System Drugs
Choińska-Mlynarczyk, Marta; Hrdlička, Vojtěch; Skopalová, J.; Šelešovská, R.; Kolivoška, Viliam; Navrátil, Tomáš
2022 - English
Drugs of the nervous system (ATC group N) belong generally to the most commonly (mis)used substances worldwide. Their determination and monitoring of these drugs and their metabolites in various body fluids or environmental matrices represent a challenge for analytical chemists. Our research is focused on the application of electrochemical methods in the monitoring of the most frequently prescribed and the newly introduced nervous system drugs of precisely specified structures and/or of defined properties. For toxicological and pharmacokinetic reasons, emphasis has been placed on investigating the reaction mechanisms of their metabolite formation. New or alternative to commonly used electroanalytical methods applicable for monitoring and characterization of target compounds in their pure state, in body fluids, wastewaters, and other environmental matrices, has been developed. To improve the chemometric parameters and sensing characteristics, attention was paid to the construction of new electrochemical sensors, detectors (e.g. screen-printed, 3D printed), or cells, based on (modified/unmodified) traditional or nontraditional materials, preferably usable at the point-of-care.
Keywords:
nervous system drugs; active pharmaceutical ingredient; metabolites; electrochemistry
Available on request at various institutes of the ASCR
Electrochemical Techniques in Monitoring of Nervous System Drugs
Drugs of the nervous system (ATC group N) belong generally to the most commonly (mis)used substances worldwide. Their determination and monitoring of these drugs and their metabolites in various body ...
NRGL provides central access to information on grey literature produced in the Czech Republic in the fields of science, research and education. You can find more information about grey literature and NRGL at service web
Send your suggestions and comments to nusl@techlib.cz
Provider
Other bases