Number of found documents: 261
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Concentrations of monosaccharide anhydrides in PM1 and PM2.5 aerosol
Mikuška, Pavel; Křůmal, Kamil; Vojtěšek, Martin; Večeřa, Zbyněk
2011 - Czech
Analysis of monosacharide anhydrides (levoglucosan, mannosan, galactosan) in two aerosol size fractions (PM1 and PM2.5) and comparison of concentrations during winter and summer campaigns in Brno and Šlapanice in 2009, identification of main emission sources. Analýza anhydridů monosacharidů (levoglukosan, mannosan, galaktosan) ve dvou velikostních frakcích aerosolu (PM1 a PM2.5) a porovnání koncentrací v průběhu zimní a letní kampaně v Brně a Šlapanicích v roce 2009, identifikace hlavních emisních zdrojů. Keywords: monosacharide anhydrides; organic tracer; biomass burning Available at various institutes of the ASCR
Concentrations of monosaccharide anhydrides in PM1 and PM2.5 aerosol

Analysis of monosacharide anhydrides (levoglucosan, mannosan, galactosan) in two aerosol size fractions (PM1 and PM2.5) and comparison of concentrations during winter and summer campaigns in Brno and ...

Mikuška, Pavel; Křůmal, Kamil; Vojtěšek, Martin; Večeřa, Zbyněk
Ústav analytické chemie, 2011

Unique exposure system for the whole body inhalation experiments with small animals
Večeřa, Zbyněk; Mikuška, Pavel; Dočekal, Bohumil; Vojta, Šimon; Míšek, Ivan; Moravec, Pavel; Smolík, Jiří
2011 - English
The especially inhalation chamber is constructed for chronic exposure studies of small animals to nanoparticles under strictly controlled conditions in frame of project „Study of transport of inhalated nano-sized particles (Pb, Cd) and their allocation in organs“. The inhalation chamber builds from a glass and stainless steel and makes possible long-term inhalation procedures (up to 60 days, 24 hours/day) with up to four discrete groups of mice population (up to 60 individuals each) or of rats population (up to 20 individuals each) under controlled illumination, temperature, relative humidity, doses (0.5 x 106 - 5 x 106 particles/cm3) and size (10-60 nm) of nano-sized particles which are synthesized via aerosol route in a hot wall tube flow reactor using metal organic precursors. Keywords: inhalation chamber; chronic exposure studies of small animals; long-term inhalation procedures Available at various institutes of the ASCR
Unique exposure system for the whole body inhalation experiments with small animals

The especially inhalation chamber is constructed for chronic exposure studies of small animals to nanoparticles under strictly controlled conditions in frame of project „Study of transport of ...

Večeřa, Zbyněk; Mikuška, Pavel; Dočekal, Bohumil; Vojta, Šimon; Míšek, Ivan; Moravec, Pavel; Smolík, Jiří
Ústav analytické chemie, 2011

Identification of sources of resuspended aerosol particles using statistic methods
Huzlík, J.; Ličbinský, R.; Mikuška, Pavel
2011 - Czech
Parallel collection of aerosol particles in size fractions PM2.5 and PM10 and street dust at the same location was performed in Ostrava and Brno during winter and summer 2009 and 2010. Identification of PM sources including resuspended PM and their contribution to overall PM concentration was done by using receptor modelling methods. Aerosoly ve velikostní frakci PM2.5 a PM10 a pouliční prach byly paralelně vzorkovány v Ostravě a Brně během zimy a léta 2009 a 2010. Zdroje aerosolů, včetně resuspendovaného prachu a jeho příspěvku k celkové koncentraci aerosolů, byly identifikovány pomocí metod receptorového modelování. Keywords: resuspension; aerosol source identification; receptor modelling Available at various institutes of the ASCR
Identification of sources of resuspended aerosol particles using statistic methods

Parallel collection of aerosol particles in size fractions PM2.5 and PM10 and street dust at the same location was performed in Ostrava and Brno during winter and summer 2009 and 2010. Identification ...

Huzlík, J.; Ličbinský, R.; Mikuška, Pavel
Ústav analytické chemie, 2011

Differentiation of Candida strains by capillary HPLC
Vykydalová, Marie; Moravcová, Dana; Horká, Marie; Růžička, F.; Kahle, Vladislav
2011 - Czech
The aim of this study was to compare chromatographic profiles of lysate of Candida parapsilosis positive and Candida parapsilosis negative using capilary high performance liquid chromatography. Cílem této práce bylo rozlišení kvasinkových kmenů porovnáním jejich chromatografických profilů lyzátů. Keywords: Candida; HPLC; biofilm Available at various institutes of the ASCR
Differentiation of Candida strains by capillary HPLC

The aim of this study was to compare chromatographic profiles of lysate of Candida parapsilosis positive and Candida parapsilosis negative using capilary high performance liquid chromatography.

Vykydalová, Marie; Moravcová, Dana; Horká, Marie; Růžička, F.; Kahle, Vladislav
Ústav analytické chemie, 2011

Electrophoretic separation of oligosaccharides with conductivity detection
Partyka, Jan; Foret, František
2011 - Czech
Improvement of separation properties of oligosaccharides by quaternary ammonium labeling. Zlepšení separačních vlastností oligosacharidů pomocí derivatizace kvartérní amoniovou značkou. Keywords: oligosaccharide; AETMA; capillary electrophoresis Available at various institutes of the ASCR
Electrophoretic separation of oligosaccharides with conductivity detection

Improvement of separation properties of oligosaccharides by quaternary ammonium labeling.

Partyka, Jan; Foret, František
Ústav analytické chemie, 2011

Using of divergent flow isoelectric focusing and capillary liquid
Duša, Filip; Moravcová, Dana; Kahle, Vladislav; Šlais, Karel
2011 - Czech
Separation of analytes from complex matrices play important role in their further identification. In this article we propose two-dimensional separation method of bovine serum albumin tryptic peptides. At the first dimension peptides are separated by divergent flow isoelectric focusing followed by reverse-phase liquid chromatography as the second dimension. Due to composition of input mixture it is possible to use autofocusing mode in first dimension. In this mode peptides are focused without addition of carrier ampholytes. Chromatograms from the second dimension were processed into contour map. Acquired data showed good separation efficiency of isoelectric focusing. Autofocusing mode enabled better resolution of peptides with close isoelectric points. Separace analytů z komplexních směsí dnes hraje významnou roli při jejich další identifikaci. V článku je navržena metoda dvoudimenzionální separace směsi tryptických peptidů hovězího sérového albuminu. V první dimenzi jsou peptidy rozděleny isoelektrickou fokusací v rozbíhavém toku a v druhé dimenzi následuje kapalinová chromatografie s reverzní fází. Díky charakteru vstupní směsi je možné u izoelektrické fokusace využít autofokusaci peptidů, tzn. fokusaci bez přídavku nosných amfolytů. Chromatogramy z druhé dimenze byly zpracovány do podoby vrstevnicové mapy. Získaná data ukázala dobrou separační účinnost izoelektrické fokusace a díky autofokusaci bylo možné rozdělit i peptidy s blízkými izoelektrickými body. Keywords: peptides; DF-IEF; RPLC Available at various institutes of the ASCR
Using of divergent flow isoelectric focusing and capillary liquid

Separation of analytes from complex matrices play important role in their further identification. In this article we propose two-dimensional separation method of bovine serum albumin tryptic ...

Duša, Filip; Moravcová, Dana; Kahle, Vladislav; Šlais, Karel
Ústav analytické chemie, 2011

Determination of organic compounds in PM1 in Brno and Šlapanice
Křůmal, Kamil; Mikuška, Pavel; Vojtěšek, Martin; Večeřa, Zbyněk
2011 - Czech
Monosaccharide anhydrides, polyaromatic hydrocarbons, hopanes, steranes and monocarboxylic acids were analysed in PM1. Contribution deals with extractions of these compounds from filters, preparations of samples, analyses by GC/MS and discussions of results of analysis. V PM1 aerosolu byly analyzovány anhydridy monosacharidů, polyaromatické uhlovodíky, hopany, sterany a monokarboxylové kyseliny. Příspěvek se zabývá extrakcemi těchto sloučenin z filtrů, přípravami vzorků, analýzami metodou GC/MS a diskusemi výsledků analýz. Keywords: organic compounds; PM1 Available at various institutes of the ASCR
Determination of organic compounds in PM1 in Brno and Šlapanice

Monosaccharide anhydrides, polyaromatic hydrocarbons, hopanes, steranes and monocarboxylic acids were analysed in PM1. Contribution deals with extractions of these compounds from filters, preparations ...

Křůmal, Kamil; Mikuška, Pavel; Vojtěšek, Martin; Večeřa, Zbyněk
Ústav analytické chemie, 2011

Analysis of saccharides and markers of wood combustion in atmospheric aerosols
Kubátková, Nela; Křůmal, Kamil; Mikuška, Pavel; Večeřa, Zbyněk
2011 - Czech
Present study deals with the analysis of saccharides (monosaccharides, disaccharides and alditols), monosaccharide anhydrides and markers of biomass and wood combustion in atmospheric aerosol and comparison of their concentrations in term of seasons. Studie se zabývá analýzou sacharidů (monosacharidy, disacharidy a alditoly), anhydridů monosacharidů a markerů spalování biomasy a dřeva v atmosférickém aerosolu a porovnáním jejich koncentrací v průběhu jednotlivých ročních období. Keywords: atmospheric aerosol PM2,5; saccharides; markers of biomass and wood combustion Available at various institutes of the ASCR
Analysis of saccharides and markers of wood combustion in atmospheric aerosols

Present study deals with the analysis of saccharides (monosaccharides, disaccharides and alditols), monosaccharide anhydrides and markers of biomass and wood combustion in atmospheric aerosol and ...

Kubátková, Nela; Křůmal, Kamil; Mikuška, Pavel; Večeřa, Zbyněk
Ústav analytické chemie, 2011

Unique exposure system for the whole body inhalation experiments with small animals
Večeřa, Zbyněk; Mikuška, Pavel; Moravec, Pavel; Smolík, Jiří
2011 - English
The especially inhalation chamber is constructed for chronic exposure studies of small animals to nanoparticles under strictly controlled conditions in frame of project „Study of transport of inhalated nano-sized particles (Pb, Cd) and their allocation in organs“. The inhalation chamber builds from a glass and stainless steel and makes possible long-term inhalation procedures (up to 60 days, 24 hours/day) with up to four discrete groups of mice population (up to 60 individuals each) or of rats population (up to 20 individuals each) under controlled illumination, temperature, relative humidity, doses (0.5 x 106 - 5 x 106 particles/cm3) and size (10-60 nm) of nano-sized particles which are synthesized via aerosol route in a hot wall tube flow reactor using metal organic precursors. Keywords: inhalation chamber; chronic exposure studies of small animals; long-term inhalation procedures Available at various institutes of the ASCR
Unique exposure system for the whole body inhalation experiments with small animals

The especially inhalation chamber is constructed for chronic exposure studies of small animals to nanoparticles under strictly controlled conditions in frame of project „Study of transport of ...

Večeřa, Zbyněk; Mikuška, Pavel; Moravec, Pavel; Smolík, Jiří
Ústav analytické chemie, 2011

Seasonal variation in chemical composition of submicron urban aerosol in Brno
Mikuška, Pavel; Křůmal, Kamil; Večeřa, Zbyněk; Vojtěšek, Martin
2011 - English
Submicron aerosol particles in the size fraction PM1 collected in Brno in winter and summer of 2009 were analysed for both selected inorganic (ions, metals) and organic components (PAHs, hopanes and steranes, monosaccharide anhydrides, monocarboxylic acids). Special attention was paid to analysis of organic molecular markers to identify the major emission sources of aerosols. Keywords: submicron aerosol; chemical composition; emission sources Available at various institutes of the ASCR
Seasonal variation in chemical composition of submicron urban aerosol in Brno

Submicron aerosol particles in the size fraction PM1 collected in Brno in winter and summer of 2009 were analysed for both selected inorganic (ions, metals) and organic components (PAHs, hopanes and ...

Mikuška, Pavel; Křůmal, Kamil; Večeřa, Zbyněk; Vojtěšek, Martin
Ústav analytické chemie, 2011

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